Leak testing and leak test machines for production

Leak Testing in production lines is done with various sensors. One of the most important things and reason for misunderstandings is the difference between the limits of these sensors and the limits of the resulting leak test machines. The detectable leak rates with leak testing machines are very often 1.000 to 100.000 times less compared to the sensor in the laboratory. The detectable leak rate of a leak test machine is more difficult to calculate because of different influence in different applications. In the following we will look to a few methods concerning their use in production lines.

Capability of the sensors?

Commonly used sensors for leak testing

Description Operator water bath testing (bubble test) Pressure difference Hydrogen (H2LT) Helium-Atmosphere (HELT-A) Ultrasonic-
Leak Tester
Helium-
Vakuum (HELT-V)
Sensor Eye Pressure sensor Semi-
conductor sensor
e.g. Wise Technology™ Ultrasound transducer Mass-
spectrometer
What is detected / measured? Gas/Air bubble approx. 1mm diameter Pressure
1 – 0,1Pa
Current Current
2·10-10A
at 5ppm He
Gas/Air bubble
< 0,1mm
diameter
Current
10-15A
Detection limit of sensor

2,6·10-5
mbar·l/s
at 20s
10-4
mbar·l/s
at 1Pa,
0,1l volume
and 10s
10-6
mbar·l/s
10-6
mbar·l/s
10-8
mbar·l/s
in 60s
10-11
mbar·l/s

We find tables as the following not very helpful. Quite the contrary: if you don’t look carefully, such tables are misleading. In many cases the detection limit of the sensor is mixed up with the detectable leak rate of a leak test machine.

What can be reached by the leak test machine under production conditions
  Leak rate in mbar·l/s
Test method
1
10-1
10-2
10-3
10-4
10-5
10-6
10-7
10-8
10-9
10-10
10-11
Operator water bath                        
Pressure difference                        
Helium Atmosphere                        
Hydrogen                         
Helium Vacuum                        
Ultrasound gas bubble detection                        

The important question is not: What can the sensor detect?
but: What can the corresponding leak tester find?

MACEAS business is mainly to build automatic leak testing equipment. This means that at least the leak test itself is done in an automatic way and not by operator. Note: also leak testing with a sniffer (either Helium or Hydrogen) is operator testing. Only if done by a robot we can talk about automatic leak testing. The result depends very strongly on how accurate the operator moves the sniffer along the areas to be tested.

In the following we only talk about automatic leak testing, as mentioned above, with just one exception: operator water bath. This is because this method is still the most common all over the world.

Operator water bath (bubble test)

Sensor:
  What is detected / measured? Detection limit of sensor
Eye Gas/Air bubble approx. 1mm diameter 2,6·10-5 mbar·l/s at 20s

Method
Part to be tested is pressurized and immersed into the water. Bubbles produced by a leak are detected by an operator looking to the water bath.

Test gas
Mainly Air, sometimes Nitrogen

Detection limit of sensor
Up to 10-5 mbar·l/s s (test in experiments but under optimised conditions, very difficult do detect this all thru a 8h shift).

Detectable leak rate in production
In dispute, but around 10-2-10-3 mbar·l/s.

Characterisation

Operator independent
–  –  –
Test result completely depend on operators decision. Strong influence from illumination, contrast and dirt in the water
Invest costs
+ +
Mainly simple water bath
Part dry after testing
–  –
Part to be tested must be immersed into a fluid
Operating and maintenance costs
+ + +
Depending on labour rates
Measuring time
+
Mainly short because the operator can watch over a long time with high concentration
Volume dependence
+ +
In principle no, but for big parts it is difficult for the operator to watch the whole area permanently
Temperature dependence
+ + +
No temperature influence
Influence of a change in volume
+ + +
No influence
Localisation
+ + +
Direct, fast localisation of leak by the operator
Test gas
+ + +
Air (sometimes Nitrogen)
Coarse leak problem
+ + +
No


Pressure difference - DPLT

Sensor:
  What is detected / measured? Detection limit of sensor
Pressure sensor Pressure 1 – 0,1Pa 10-4 mbar·l/s at 1Pa, 0,1l volume and 10s

Method
Part to be tested and reference volume is pressurised. The leakage is detected in an indirect way by measuring the pressure difference between the part to be tested and the reference volume in case of a leak.

Test gas
Air, sometimes Nitrogen.

Detection limit of sensor
Pressure differences in the range of 0,1 – 1Pa

Detectable leak rates in production
Up to 10-2 mbar·l/s (very strongly depending on the test volume)

Characterisation

Operator independent
+ + +
Yes
Invest costs
+ + +
Mostly the cheapest test method (if it does not work reliable, a waste of money!)
Part dry
+ + +
Yes
Operating- and maintenance costs
+ +
Periodic calibration required
Measuring time
+ +
Mainly short, because long measuring times rise the probability of temperature influence
Volume dependence
–  –  –
The same leak cause completely different pressure differences. For a big volume there is just a small change. For a very small volume there is a much higher change in pressure
Temperature dependence
–  –  –
Typically the temperature influence is much bigger then the detection limit of the pressure sensor. In addition the temperature influence rise with the test pressure
Influence of a change in volume
–  –  –
If the test volume is changing during the measurement this causes also a change of pressure
Localisation
–  –  –
No localisation
Test gas
+ + +
Air, sometimes Nitrogen
Coarse leak problem
+ + +
Yes, when used to completely closed parts (pressure increase in chamber)

Hydrogen – H2LT

Sensor:
  What is detected / measured? Detection limit of sensor
Semiconductor sensor Current 10-6 mbar·l/s

Method
Part to be tested must be put in a chamber, evacuated (no high vacuum required) and pressurised with test gas mixture, typically 5% Hydrogen and 95% Nitrogen. If there is a leakage the concentration of the test gas in the measuring chamber will rise. The rise of concentration is measured by the semiconductor sensor.

Test gas
Forming gas (Hydrogen-Nitrogen-mixture, 5% Nitrogen )

Detection limit of sensor
10-6 mbar·l/s

Detectable leak rate in production
More or less in the range around 10-2mbar·l/s (depending on the volume in the test chamber)

Characterisation

Operator independent
+ + +
Yes 
Invest costs
+
No vacuum chamber required (normal chamber can be used) but part has to be evacuated before filling with the test gas to get homogeneous distribution of test gas
Part dry
+ + +
Yes
Operating- and maintenance costs
+
Periodic calibration required, maintenance of vacuum pump(s), costs for test gas low
Measuring time
– 
Strongly depending on the chamber volume. For big volumes the increase of test gas concentration is very low.
Volume dependence
–  –  –
See measuring time.
Temperature dependence
+ + +
No influence under normal environment conditions
Influence of a change in volume
+ + +
No influence
Localisation
–  –  –
No localisation
Test gas
  –
Forming gas (Hydrogen-Nitrogen mixture)
Coarse leak problem
–  –  –
Contamination of chamber and environment due to coarse leaks

Helium at atmosphere - HELT-A

Sensor:
  What is detected / measured? Detection limit of sensor
e.g. Wise Technology™ Current 2·10-10A at 5ppm He 10-6 mbar·l/s

Method
Part to be tested must be put in a chamber, evacuated (no high vacuum required) and pressurised with test gas (mixture). If there is a leakage the concentration of the test gas in the measuring chamber will rise. The rise of concentration is measured by the Helium sensor.

Test gas
Helium, Helium-Air mixture, He-Nitrogen-mixture

Detection limit of sensor
10-6 mbar·l/s

Detectable leak rate in production
More ore less in the range around of 10-2mbar·l/s (strongly depending on chamber volume)

Characterisation

Operator independent
+ + +
Yes
Invest costs
+
No vacuum chamber required (normal chamber can be used) but part has to be evacuated before filling with the test gas to get homogeneous distribution of test gas
Part dry
+ + +
Yes
Operating- and maintenance costs
+
Periodic calibration required, maintenance of vacuum pump(s), test gas
Measuring time
Strongly depending on the chamber volume. For big volumes the increase of test gas concentration is very low
Volume dependence
–  –  –
See measuring time
Temperature dependence
+ + +
No influence under normal environment conditions
Influence of a change in volume
+ + +
No influence
Localisation
–  –  –
No localisation
Test gas
–  – 
Helium, Helium mixture
Coarse leak problem
–  –  –
Contamination of chamber and environment due to coarse leaks

Ultrasonic Leak Tester - USLT

Sensor:
  What is detected / measured? Detection limit of sensor
Ultrasound transducer Gas/Air bubble< 0,1mm diameter 10-8 mbar·l/s in 60s

Method
Part to be tested is pressurised and immersed into the water. Raising bubbles are detected and localised by an ultrasonic system.

Test gas
Air, sometimes Nitrogen

Detection limit of sensor
Up to 10-8 mbar·l/s

Detectable leak rates in production
Up to 10-5 mbar·l/s

Characterisation

Operator independent
+ + +
Yes
Invest costs
–  – 
Ultrasound technology requires more sophisticated water baths and some design requirements for machine building
Part dry
–  – 
Part must be immersed into a liquid
Operating- and maintenance costs
+ + +
Very low
Measuring time
+
Only according to leak rate
Volume dependence
+ + +
No influence of volume
Temperature dependence
+ + +
No influence of temperature
Influence of a change in volume
+ + +
No influence
Localisation
+ + +
Direct, fast localisation of leak bubbles by ultrasonic system (additional immediately analyses by operator possible)
Test gas
+ + +
Air, sometimes Nitrogen
Coarse leak problem
+ + +
No problem

Helium Vacuum chamber - HELT-V

Sensor:
  What is detected / measured? Detection limit of sensor
Mass-spectrometer Current
10-15 A
<1·10-11 mbar·l/s

Method
Part to be tested and chamber must be evacuated. Part is filled with test gas. If due to leakage the test gas expands into the chamber, the mass spectrometer detects the Helium.

Test gas
Helium, Helium-Air mixture, He-Nitrogen mixture.

Detection limit of sensor
10-11 mbar·l/s.

Detectable leak rates in production
Up to 10-7 mbar·l/s.

Characterisation

Operator independent
+ + +
Yes
Invest costs
–  –  –
Vacuum chamber required, dimensions of pumps must be good enough to compensate environmental variations (e.g.. high humidity)
Part dry
+ + +
Yes
Operating- and maintenance costs
–  –  –
Periodic calibration required, maintenance for vacuum technology, test gas costs.
Measuring time
+
Measuring time itself mainly short. For big chamber volume the time to reach the required vacuum can be high
Volume dependence
+
See measuring time
Temperature dependence
+ + +
No influence
Influence of a change in volume
+ + +
No influence
Localisation
–  –  –
No localisation
Test gas
–  – 
Helium, Helium mixture
Coarse leak problem
–  –  –
Contamination of chamber and environment due to coarse leaks


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Fon +49 (0) 4497 / 92190-20 · Fax +49 (0) 4497 / 92190-19 · info@maceas.com · www.maceas.com
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